Press release

 

New mechanical behavior observed for nanocrystalline copper

Paris, April 11, 2003

 

Researchers from the Chemical Metallurgy Research Center of the CNRS (CECM, Vitry-sur-Seine, France) and the Laboratoire d’Ingénierie des Matériaux et des Hautes Pressions of the CNRS (LIMHP, Villetaneuse, France) have just demonstrated the exceptional mechanical properties of nanocrystalline copper. This material displays a near-perfect elastoplastic behavior never before observed.
This research appears in the April 11, 2003, issue of the journal, Science.


The CECM and LIMHP teams carried out tensile tests on fully dense large-scale bulk nanocrystalline samples, a material that has a grain size smaller than the characteristic length scales normally encountered: about one hundred nanometers as opposed to several microns1 . These tests consist of following the evolution of the deformation of the material depending on the applied stress. These are the first tensile tests on a material with such fine grains (an average of 80 nanometers) made on representative tensile testing samples (35 mm long with a diameter of 3.5 mm). Two special techniques were used to obtain this type of material: the massive production of ultrafine metal powder using a cryogenic evaporation-condensation technique (developed at the CECM) and differential cold extrusion (developed at the LIMHP).

The mechanical properties obtained are exceptional: nanocrystalline copper is three times more resistant than normal copper and deforms homogeneously with no apparent necking by a steady deformation flow until sample failure occurs. Researchers were thus able to observe a near-perfect electroplasticity for the first time. Deformation normally takes place heterogeneously in traditional materials, increasing with applied stress and leading to premature crack propagation and, ultimately, failure.

This behavior could be explained by high atomic diffusion and the small size of the grains which would make it possible to activate superplastic-type mechanisms at room temperature: the grains would slide around in a fluid flow. Superplasticity occurs at higher temperatures for traditional materials. The behavior observed opens some very interesting prospects for plastic formation of materials at room temperature.

1 - A nanometer is equivalent to one thousandth of a micron.




Researchers contact:
Chemical Sciences Department
(CECM)

Yannick Champion
Tel: +33 1 56 70 30 30
e-mail:
yannick.champion@glvt-cnrs.fr

Engineering Sciences Department
(LIMHP)

Patrick Langlois
Tel: +33 1 49 40 34 17/34 27
E-mail: langlois@limhp.univ-paris13.fr


Press contact :
Muriel Ilous
Tel : +33 1 44 96 43 09
e-mail : muriel.ilous@cnrs-dir.fr